Technology Process of 1-methoxy-4-(3-(3-(4-nitrophenyl)prop-2-ynylsulfonyl)prop-1-ynyl)benzene
There total 10 articles about 1-methoxy-4-(3-(3-(4-nitrophenyl)prop-2-ynylsulfonyl)prop-1-ynyl)benzene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
at 20 ℃;
for 2h;
Inert atmosphere;
Cooling with ice;
DOI:10.1021/ol102861j
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: ethanol; pyridinium p-toluenesulfonate / 20 °C
2.1: carbon tetrabromide; triphenylphosphine / dichloromethane / Inert atmosphere; Cooling with ice
3.1: methanol; potassium carbonate / 0.25 h / -20 °C / Inert atmosphere
3.2: 3 h / -20 - 20 °C / Inert atmosphere
4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 20 °C / Inert atmosphere; Cooling with ice
With
methanol; ethanol; carbon tetrabromide; pyridinium p-toluenesulfonate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine;
In
dichloromethane;
DOI:10.1021/ol102861j
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: methanol; potassium carbonate / 0.25 h / -20 °C / Inert atmosphere
1.2: 3 h / -20 - 20 °C / Inert atmosphere
2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 20 °C / Inert atmosphere; Cooling with ice
With
methanol; potassium carbonate; 3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
DOI:10.1021/ol102861j
