4-N'-hydroxyamidinobenzyl 4-N'-hydroxyamidinophenyl ether

Base Information

• Chemical Name: 4-N'-hydroxyamidinobenzyl 4-N'-hydroxyamidinophenyl ether
• CAS No.: 1456777-87-9
• Molecular Formula: C₁₅H₁₆N₄O₃
• Molecular Weight: 300.317
• Mol file: 1456777-87-9.mol

Synonyms:4-N'-hydroxyamidinobenzyl 4-N'-hydroxyamidinophenyl ether

Chemical Property of 4-N'-hydroxyamidinobenzyl 4-N'-hydroxyamidinophenyl ether

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 4-N'-hydroxyamidinobenzyl 4-N'-hydroxyamidinophenyl ether

There total 3 articles about 4-N'-hydroxyamidinobenzyl 4-N'-hydroxyamidinophenyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

4-cyanobenzyloxy-4'-cyanophenyl ether (57928-92-4) → 4-N'-hydroxyamidinobenzyl 4-N'-hydroxyamidinophenyl ether (1456777-87-9)

Guidance literature:

With hydroxylamine hydrochloride; potassium tert-butylate; In dimethyl sulfoxide;

DOI:10.1016/j.ejmech.2013.06.033

Reference yield:

4-cyanophenol (767-00-0) → 4-N'-hydroxyamidinobenzyl 4-N'-hydroxyamidinophenyl ether (1456777-87-9)

Guidance literature:

Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 110 °C

1.2: 1 h

2.1: hydroxylamine hydrochloride; potassium tert-butylate / dimethyl sulfoxide

With hydroxylamine hydrochloride; potassium tert-butylate; potassium carbonate; In dimethyl sulfoxide; N,N-dimethyl-formamide;

DOI:10.1016/j.ejmech.2013.06.033

Reference yield:

4-cyanobenzyl bromide (17201-43-3) → 4-N'-hydroxyamidinobenzyl 4-N'-hydroxyamidinophenyl ether (1456777-87-9)

Guidance literature:

Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 110 °C

1.2: 1 h

2.1: hydroxylamine hydrochloride; potassium tert-butylate / dimethyl sulfoxide

With hydroxylamine hydrochloride; potassium tert-butylate; potassium carbonate; In dimethyl sulfoxide; N,N-dimethyl-formamide;

DOI:10.1016/j.ejmech.2013.06.033

upstream raw materials:

4-cyanophenol

4-cyanobenzyl bromide

4-cyanobenzyloxy-4'-cyanophenyl ether

Refernces