Technology Process of 3-(4-hydroxy-3-methoxyphenyl)propanamide
There total 5 articles about 3-(4-hydroxy-3-methoxyphenyl)propanamide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
ferrous ammonium sulphate hexahydrate; isopropyl β-D-thiogalactopyranoside;
In
aq. phosphate buffer;
at 37 ℃;
for 48h;
DOI:10.1002/anie.201403148
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydroxide / 2 h / 0 - 20 °C / Inert atmosphere
2: triethylamine / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere
3: ammonium hydroxide / 0 - 20 °C / Inert atmosphere
4: ferrous ammonium sulphate hexahydrate; isopropyl β-D-thiogalactopyranoside / aq. phosphate buffer / 48 h / 37 °C
With
ammonium hydroxide; ferrous ammonium sulphate hexahydrate; isopropyl β-D-thiogalactopyranoside; triethylamine; sodium hydroxide;
In
tetrahydrofuran; aq. phosphate buffer;
DOI:10.1002/anie.201403148
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere
2: ammonium hydroxide / 0 - 20 °C / Inert atmosphere
3: ferrous ammonium sulphate hexahydrate; isopropyl β-D-thiogalactopyranoside / aq. phosphate buffer / 48 h / 37 °C
With
ammonium hydroxide; ferrous ammonium sulphate hexahydrate; isopropyl β-D-thiogalactopyranoside; triethylamine;
In
tetrahydrofuran; aq. phosphate buffer;
DOI:10.1002/anie.201403148