tetrakis(trimethylstannyl)distibane

Base Information

• Chemical Name: tetrakis(trimethylstannyl)distibane
• CAS No.: 68354-51-8
• Molecular Formula: C₁₂H₃₆Sb₂Sn₄
• Molecular Weight: 898.758
• Mol file: 68354-51-8.mol

Synonyms:tetrakis(trimethylstannyl)distibane

Chemical Property of tetrakis(trimethylstannyl)distibane

Chemical Property:

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Technology Process of tetrakis(trimethylstannyl)distibane

There total 2 articles about tetrakis(trimethylstannyl)distibane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

benzylbis(trimethylstannyl)stibane (124593-75-5) → tetrakis(trimethylstannyl)distibane (68354-51-8) + 1,1'-(1,2-ethanediyl)bisbenzene (103-29-7)

Guidance literature:

In 1,2-dimethoxyethane; Irradiation (UV/VIS); Ar atmosphere; irradiation (diffuse day light, 1 week);

Reference yield: 47.0%

tris(trimethylstannyl)stibine (7029-29-0) → bis(trimethyltin)oxide (1692-18-8) + tetrakis(trimethylstannyl)distibane (68354-51-8) + trimethyltin(IV) hydroxide (56-24-6)

Guidance literature:

With oxygen; In neat (no solvent); stibane left in air for 3 d; suspending in Ar-satd. acetone, decanting, recrystn. of red residue from toluene (2nd and 3rd product isolated from acetone suspn.); elem. anal.;

upstream raw materials:

tris(trimethylstannyl)stibine

benzylbis(trimethylstannyl)stibane

Refernces