Technology Process of C22H23ClO3
There total 3 articles about C22H23ClO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate; 1-methyl-3-methylimidazol-3-ium dimethyl phosphate;
In
toluene;
at 110 ℃;
for 0.833333h;
Inert atmosphere;
Microwave irradiation;
DOI:10.1021/jm3008213
- Guidance literature:
-
Multi-step reaction with 3 steps
1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / diethyl ether / 6 h / 0 - 20 °C
2: sodium iodide; aluminum (III) chloride / acetonitrile; dichloromethane / 1 h / 0 - 20 °C
3: potassium carbonate; 1-methyl-3-methylimidazol-3-ium dimethyl phosphate / toluene / 0.83 h / 110 °C / Inert atmosphere; Microwave irradiation
With
aluminum (III) chloride; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; potassium carbonate; sodium iodide; 1-methyl-3-methylimidazol-3-ium dimethyl phosphate;
In
diethyl ether; dichloromethane; toluene; acetonitrile;
DOI:10.1021/jm3008213
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium iodide; aluminum (III) chloride / acetonitrile; dichloromethane / 1 h / 0 - 20 °C
2: potassium carbonate; 1-methyl-3-methylimidazol-3-ium dimethyl phosphate / toluene / 0.83 h / 110 °C / Inert atmosphere; Microwave irradiation
With
aluminum (III) chloride; potassium carbonate; sodium iodide; 1-methyl-3-methylimidazol-3-ium dimethyl phosphate;
In
dichloromethane; toluene; acetonitrile;
DOI:10.1021/jm3008213
