Technology Process of 3,4,5-trihydroxyphenethyl methyl carbonate
There total 4 articles about 3,4,5-trihydroxyphenethyl methyl carbonate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: copper(I) bromide / methanol / 20 °C / Green chemistry
1.2: 3 h / 90 °C / Green chemistry
2.1: carbonic acid dimethyl ester / 24 h / 20 °C
3.1: boron tribromide / dichloromethane / -40 °C
With
boron tribromide; carbonic acid dimethyl ester; copper(I) bromide;
In
methanol; dichloromethane;
DOI:10.1007/s00044-012-0052-8
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: carbonic acid dimethyl ester; sodium bromide; potassium peroxymonosulfate / water / 20 °C / Green chemistry
2.1: copper(I) bromide / methanol / 20 °C / Green chemistry
2.2: 3 h / 90 °C / Green chemistry
3.1: carbonic acid dimethyl ester / 24 h / 20 °C
4.1: boron tribromide / dichloromethane / -40 °C
With
potassium peroxymonosulfate; boron tribromide; carbonic acid dimethyl ester; sodium bromide; copper(I) bromide;
In
methanol; dichloromethane; water;
DOI:10.1007/s00044-012-0052-8
