C₁₄H₃₂Cl₂O₅Si₂

Base Information

• Chemical Name: C₁₄H₃₂Cl₂O₅Si₂
• CAS No.: 158588-47-7
• Molecular Formula: C₁₄H₃₂Cl₂O₅Si₂
• Molecular Weight: 407.482
• Mol file: 158588-47-7.mol

Synonyms:C₁₄H₃₂Cl₂O₅Si₂

Chemical Property of C₁₄H₃₂Cl₂O₅Si₂

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

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Technology Process of C₁₄H₃₂Cl₂O₅Si₂

There total 3 articles about C₁₄H₃₂Cl₂O₅Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(3-chloropropyl)triethoxysilane (5089-70-3) → C14H32Cl2O5Si2 (158588-47-7) + C14H34O5S2Si2 + 3-Mercaptopropyltriethoxysilane (14814-09-6) + bis-[γ-(triethoxysilyl)propyl]sulfide (60764-86-5) + 4,4,13,13-tetraethoxy-3,14-dioxa-8,9-dithia-4,13-disilahexadecane (56706-10-6)

Guidance literature:

With sodium hydrogensulfide; In ethanol; at 90 - 100 ℃; for 2 - 4h; Conversion of starting material;

Reference yield:

ethanol (64-17-5) + 3-chloropropyltrichlorosilane (2550-06-3) + (3-chloropropyl)triethoxysilane (5089-70-3) → C14H32Cl2O5Si2 (158588-47-7) + C14H34O5S2Si2 + 3-Mercaptopropyltriethoxysilane (14814-09-6) + bis-[γ-(triethoxysilyl)propyl]sulfide (60764-86-5) + 4,4,13,13-tetraethoxy-3,14-dioxa-8,9-dithia-4,13-disilahexadecane (56706-10-6)

Guidance literature:

With sodium hydrogensulfide; at 90 - 100 ℃; for 2 - 4h; Conversion of starting material;

Reference yield:

(3-chloropropyl)triethoxysilane (5089-70-3) + carbon dioxide (124-38-9,18923-20-1) → C14H32Cl2O5Si2 (158588-47-7) + Diethyl carbonate (105-58-8,76619-83-5)

Guidance literature:

With zirconium(IV) ethoxide; at 180 ℃; under 37503.8 Torr; Autoclave;

DOI:10.1002/cssc.202002471

upstream raw materials:

(3-chloropropyl)triethoxysilane

ethanol

3-chloropropyltrichlorosilane

carbon dioxide

Downstream raw materials:

(3-chloropropyl)triethoxysilane

Refernces

• 1、 -. "Process for the preparation of (mercaptoorganyl)-alkoxysilanen". Page/Page column 9; 10. . Retrieved 2008/06/13.