C₃₃H₃₈BrFN₂O₆

Base Information Edit

Chemical Name:C₃₃H₃₈BrFN₂O₆
CAS No.:1311411-84-3
Molecular Formula:C₃₃H₃₈BrFN₂O₆
Molecular Weight:657.577
Hs Code.:
Mol file:1311411-84-3.mol

C<sub>33</sub>H<sub>38</sub>BrFN<sub>2</sub>O<sub>6</sub>

Synonyms:C₃₃H₃₈BrFN₂O₆

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Chemical Property of C₃₃H₃₈BrFN₂O₆ Edit

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Technology Process of C₃₃H₃₈BrFN₂O₆

There total 28 articles about C₃₃H₃₈BrFN₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1311411-82-1
C₃₀H₄₃BrFNO₅Si

: 138603-50-6
cis-4-amino-3-chromanol

: 1311411-84-3
C₃₃H₃₈BrFN₂O₆

Guidance literature:: C₃₀H₄₃BrFNO₅Si; cis-4-amino-3-chromanol; With triethylamine; HATU; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

With tetrabutyl ammonium fluoride; In tetrahydrofuran; N,N-dimethyl-formamide; at 50 ℃;

With water; sodium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 49701-11-3
8-chloro-2,3-dihydro-4H-1-benzopyran-4-one

: 1311411-84-3
C₃₃H₃₈BrFN₂O₆

Guidance literature:: Multi-step reaction with 7 steps

1.1: bromine / dichloromethane / 0.5 h / Reflux

2.1: sodium tetrahydroborate; methanol / 0.5 h / 0 - 20 °C

3.1: sulfuric acid / 45 - 50 °C

4.1: water / acetonitrile / 48 h / Reflux

5.1: Chiralpak Daicel^.(R). AD / acetonitrile / Resolution of racemate

6.1: hydrogen / palladium on carbon / 760.05 Torr

7.1: triethylamine; HATU / N,N-dimethyl-formamide / 1 h / 20 °C

7.2: 50 °C

With methanol; sodium tetrahydroborate; sulfuric acid; water; hydrogen; bromine; triethylamine; HATU; palladium on carbon; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 95-57-8
2-monochlorophenol

: 1311411-84-3
C₃₃H₃₈BrFN₂O₆

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium hydroxide / water / 4.5 h / Reflux

1.2: 20 °C

2.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 20 °C / Cooling with ice

3.1: aluminum (III) chloride / dichloromethane / 20 °C

4.1: bromine / dichloromethane / 0.5 h / Reflux

5.1: sodium tetrahydroborate; methanol / 0.5 h / 0 - 20 °C

6.1: sulfuric acid / 45 - 50 °C

7.1: water / acetonitrile / 48 h / Reflux

8.1: Chiralpak Daicel^.(R). AD / acetonitrile / Resolution of racemate

9.1: hydrogen / palladium on carbon / 760.05 Torr

10.1: triethylamine; HATU / N,N-dimethyl-formamide / 1 h / 20 °C

10.2: 50 °C

With methanol; aluminum (III) chloride; sodium tetrahydroborate; oxalyl dichloride; sulfuric acid; water; hydrogen; bromine; triethylamine; HATU; sodium hydroxide; palladium on carbon; N,N-dimethyl-formamide; In dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;