diallylethylphosphine

Base Information

• Chemical Name: diallylethylphosphine
• CAS No.: 857684-82-3
• Molecular Formula: C₈H₁₅P
• Molecular Weight: 142.181
• Mol file: 857684-82-3.mol

Synonyms:diallylethylphosphine

Chemical Property of diallylethylphosphine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of diallylethylphosphine

There total 1 articles about diallylethylphosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

ethylmagnesium bromide (925-90-6) + cis-2,10-dimethyl-<1,2,3>benzothiadiphospholo<2,3-b><1,2,3>benzothiadiphosphole (119841-34-8,127780-84-1) + allylmagnesium bromide (1730-25-2) → diallylethylphosphine (857684-82-3) + 4-methyl-2-[(5-methyl-2-sulfanylphenyl)phosphanyl]benzenethiol (736137-64-7)

Guidance literature:

cis-2,10-dimethyl-<1,2,3>benzothiadiphospholo<2,3-b><1,2,3>benzothiadiphosphole; allylmagnesium bromide; In tetrahydrofuran; for 0.0833333h;

ethylmagnesium bromide; In tetrahydrofuran;

DOI:10.1021/jo0502145

Reference yield: 88.0%

ethylphenylphosphinous cyanide (74626-63-4) + diallylethylphosphine (857684-82-3) → [(NCCH2CH2)PhP(CH2)3]2PEt

Guidance literature:

2,2'-azobis(isobutyronitrile); for 22h; Photolysis;

upstream raw materials:

ethylmagnesium bromide

cis-2,10-dimethyl-<1,2,3>benzothiadiphospholo<2,3-b><1,2,3>benzothiadiphosphole

allylmagnesium bromide

Refernces