4-(Dodecyloxy)aniline

Base Information

• Chemical Name: 4-(Dodecyloxy)aniline
• CAS No.: 65039-19-2
• Molecular Formula: C18H31 N O
• Molecular Weight: 277.45
• Hs Code.: 2922299090
• European Community (EC) Number: 653-236-7
• DSSTox Substance ID: DTXSID80393063
• Nikkaji Number: J1.401.716J
• Wikidata: Q82191677
• Mol file: 65039-19-2.mol

Synonyms:4-(dodecyloxy)aniline;65039-19-2;4-dodecoxyaniline;4-n-dodecyloxyaniline;4-dodecyloxyaniline;p-Dodecyloxyaniline;Benzenamine, 4-(dodecyloxy)-;SCHEMBL4738920;DTXSID80393063;VXMYUOSDIMLATO-UHFFFAOYSA-N;MFCD00025323;AKOS012711446;A834953

Chemical Property of 4-(Dodecyloxy)aniline

Chemical Property:

• Vapor Pressure: 1.3E-06mmHg at 25°C
• Refractive Index: 1.504
• Boiling Point: 400.1°C at 760 mmHg
• Flash Point: 180.1°C
• PSA: 35.25000
• Density: 0.933g/cm³
• LogP: 6.14970
• XLogP3: 6.9
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 12
• Exact Mass: 277.240564612
• Heavy Atom Count: 20
• Complexity: 200

Purity/Quality:

99% ^*data from raw suppliers

4-(DODECYLOXY)ANILINE Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCCCCCCOC1=CC=C(C=C1)N

Technology Process of 4-(Dodecyloxy)aniline

There total 17 articles about 4-(Dodecyloxy)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4-dodecyloxy-1-nitrobenzene (65039-18-1) → 4-(dodecyloxy)aniline (65039-19-2)

Guidance literature:

With hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; for 1h; under 2327.17 Torr;

DOI:10.1021/ja045587m

Reference yield: 99.0%

N-(4-(dodecyloxy)phenyl)acetamide (95705-65-0) → 4-(dodecyloxy)aniline (65039-19-2)

Guidance literature:

With hydrogenchloride; In water; for 24h; Reflux;

DOI:10.1021/ma902460c

Reference yield: 87.0%

4-acetaminophenol (103-90-2,8055-08-1) + 1-dodecylbromide (143-15-7) → 4-(dodecyloxy)aniline (65039-19-2)

Guidance literature:

4-acetaminophenol; 1-dodecylbromide; With potassium carbonate; In acetone; for 48h; Reflux;

With hydrogenchloride; ethanol; for 4h; Reflux;

DOI:10.1155/2017/2378186

upstream raw materials:

4-dodecyloxy-1-nitrobenzene

N-(4-(dodecyloxy)phenyl)acetamide

4-acetaminophenol

1-dodecylbromide

Downstream raw materials:

N-<4-<10-<(2-Hydroxyethyl)dimethylammonio>decyloxy>salicylidene>-4-(dodecyloxy)aniline bromide

4-<(4-(dodecyloxy)phenyl)azo>phenol

(E)-tetrakis(4-dodecyloxyphenyl) 5,5'-(diazene-1,2-diyl)diisophthalamide

2,5-bis[(4-dodecyloxyphenyl)aminocarbonyl]styrene

Refernces

• 1、 ?a?lar, Fatma P?nar,Akda?-K?l??, Huriye,Eran, Belk?z Bilgin,Ocak, Hale. "Chiral polymorphism in new imine based rod-like liquid crystals". . . Retrieved 2020/07/06.
• 2、 Yuan, Lin,Shen, Jie,Ye, Ruijuan,Chen, Feng,Zeng, Huaqiang. "Structurally simple trimesic amides as highly selective anion channels". supporting information. p. 4797 - 4800. Retrieved 2019/05/02.