4-iodo-1H-imidazolium chloride

Base Information

• Chemical Name: 4-iodo-1H-imidazolium chloride
• CAS No.: 1443425-57-7
• Molecular Formula: C₃H₃IN₂*ClH
• Molecular Weight: 230.436
• Mol file: 1443425-57-7.mol

Synonyms:4-iodo-1H-imidazolium chloride

Chemical Property of 4-iodo-1H-imidazolium chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-iodo-1H-imidazolium chloride

There total 2 articles about 4-iodo-1H-imidazolium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

4,5-diiodo-1H-imidazole (15813-09-9) + phenylboronic acid (98-80-6) → 4-iodo-1H-imidazolium chloride (1443425-57-7) + 4-Phenylimidazole (670-95-1)

Guidance literature:

4,5-diiodo-1H-imidazole; phenylboronic acid; With dipotassium hydrogenphosphate; palladium diacetate; XPhos; In methanol; water; at 120 ℃; Inert atmosphere; Microwave irradiation;

With hydrogenchloride; In methanol; water; Inert atmosphere;

DOI:10.1002/adsc.201300395

Reference yield:

4,5-diiodo-1H-imidazole (15813-09-9) + phenylboronic acid (98-80-6) → 4,5-diphenyl-1H-imidazole (668-94-0) + 4-iodo-1H-imidazolium chloride (1443425-57-7)

Guidance literature:

4,5-diiodo-1H-imidazole; phenylboronic acid; With dipotassium hydrogenphosphate; tetrabutylammomium bromide; palladium diacetate; XPhos; In methanol; water; at 100 ℃; for 1h; Inert atmosphere; Microwave irradiation;

With hydrogenchloride; In methanol; water; Temperature; Inert atmosphere;

DOI:10.1002/adsc.201300395

Reference yield: 61.0%

4-iodo-1H-imidazolium chloride (1443425-57-7) → 4-iodoimidazole (71759-89-2)

Guidance literature:

With sodium hydrogencarbonate; In water; pH=Ca. 6;

DOI:10.1002/adsc.201200723

upstream raw materials:

4,5-diiodo-1H-imidazole

phenylboronic acid

Downstream raw materials:

4-iodoimidazole

Refernces