2-(methoxymethyl)cyclohexa-2,5-diene-1,4-dione oxime

Base Information

• Chemical Name: 2-(methoxymethyl)cyclohexa-2,5-diene-1,4-dione oxime
• CAS No.: 1380070-69-8
• Molecular Formula: C₈H₁₀N₂O₃
• Molecular Weight: 182.179
• Mol file: 1380070-69-8.mol

Synonyms:2-(methoxymethyl)cyclohexa-2,5-diene-1,4-dione oxime

Chemical Property of 2-(methoxymethyl)cyclohexa-2,5-diene-1,4-dione oxime

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(methoxymethyl)cyclohexa-2,5-diene-1,4-dione oxime

There total 7 articles about 2-(methoxymethyl)cyclohexa-2,5-diene-1,4-dione oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2-Methoxymethyl-benzochinon-1,4-4-oxim (22802-51-3) → 2-(methoxymethyl)cyclohexa-2,5-diene-1,4-dione oxime (1380070-69-8)

Guidance literature:

With hydroxylamine hydrochloride; potassium carbonate; In ethanol; for 4h; Reflux;

Reference yield:

2-methoxyacetic acid (625-45-6) + p-benzoquinone (106-51-4) → p-benzoquinone dioxime (105-11-3,6133-83-1,6421-98-3) + 2-(methoxymethyl)cyclohexa-2,5-diene-1,4-dione oxime (1380070-69-8)

Guidance literature:

2-methoxyacetic acid; p-benzoquinone; With ammonium persulfate; silver nitrate; In water; at 65 ℃; for 0.25h;

With sodium acetate; In ethanol; for 12h; Reflux;

Reference yield:

2-(methoxymethyl)-1,4-benzoquinone (7715-19-7) → 2-(methoxymethyl)cyclohexa-2,5-diene-1,4-dione oxime (1380070-69-8)

Guidance literature:

With hydroxylamine; calcium carbonate; In ethanol; for 12h; Reflux;

upstream raw materials:

salicylic alcohol

2-(methoxymethyl)phenol

2-Methoxymethyl-benzochinon-1,4-4-oxim

3-Hydroxybenzyl alcohol

Downstream raw materials:

2-(methoxymethyl)-p-phenylenediamine

Refernces

• 1、 -. "PROCESS FOR THE PREPARATION OF 2-METHOXYMETHYL-1,4-BENZENEDIAMINE, ITS DERIVATIVES THEREOF AND THE SALTS THEREOF". . . Retrieved 2012/06/16.