Technology Process of C15H19N3O4
There total 5 articles about C15H19N3O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
acetonitrile;
at 0 - 20 ℃;
for 24h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: triethylamine / acetonitrile / 24 h / 0 - 20 °C / Inert atmosphere
2.1: triethylamine / dichloromethane / 14 h / 0 - 20 °C / Inert atmosphere
3.1: dimethyl sulfoxide / 21 h / 80 °C / Inert atmosphere
4.1: hydrogenchloride; water / 4.5 h / Reflux
4.2: 7 h / 0 - 20 °C
4.3: pH 2
5.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / acetonitrile / 24 h / 0 - 20 °C / Inert atmosphere
With
hydrogenchloride; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; dimethyl sulfoxide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: triethylamine / dichloromethane / 14 h / 0 - 20 °C / Inert atmosphere
2.1: dimethyl sulfoxide / 21 h / 80 °C / Inert atmosphere
3.1: hydrogenchloride; water / 4.5 h / Reflux
3.2: 7 h / 0 - 20 °C
3.3: pH 2
4.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / acetonitrile / 24 h / 0 - 20 °C / Inert atmosphere
With
hydrogenchloride; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; dimethyl sulfoxide; acetonitrile;