Benzaldehyde, 3,6-difluoro-2-hydroxy- (9CI)

Base Information

• Chemical Name: Benzaldehyde, 3,6-difluoro-2-hydroxy- (9CI)
• CAS No.: 502762-92-7
• Molecular Formula: C7H4F2O2
• Molecular Weight: 158.104
• Hs Code.: 2912490090
• Mol file: 502762-92-7.mol

Synonyms:Benzaldehyde, 3,6-difluoro-2-hydroxy- (9CI);3,6-Difluorosalicylaldehyde, 98+%;3,6-Difluoro-2-formylphenol, 3,6-Difluorosalicylaldehyde;3,6-Difluorosalicylaldehyde;3,6-Dfluoro-2-hydroxybenzaldehyde

Chemical Property of Benzaldehyde, 3,6-difluoro-2-hydroxy- (9CI)

Chemical Property:

• Vapor Pressure: 0.58mmHg at 25°C
• Refractive Index: 1.559
• Boiling Point: 182.92 °C at 760 mmHg
• Flash Point: 64.428 °C
• Density: 1.465 g/cm³
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

98%min ^*data from raw suppliers

3,6-Difluoro-2-hydroxybenzaldehyde ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 3,6-DIFLUORO-2-HYDROXYBENZALDEHYDE is a useful research chemical.

Technology Process of Benzaldehyde, 3,6-difluoro-2-hydroxy- (9CI)

There total 1 articles about Benzaldehyde, 3,6-difluoro-2-hydroxy- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 3,6-difluoro-2-hydroxybenzaldehyde (502762-92-7)

Guidance literature:

Reference yield: 91.0%

3,6-difluoro-2-hydroxybenzaldehyde (502762-92-7) + prenyl bromide (870-63-3) → 3,6-difluoro-2-[(3-methylbut-2-en-1-yl)oxy]benzaldehyde (1412443-27-6)

Guidance literature:

With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; at 20 ℃; for 2.5h; Inert atmosphere;

DOI:10.1016/j.tet.2012.08.087

Reference yield:

3,6-difluoro-2-hydroxybenzaldehyde (502762-92-7) + Chloromethyltrimethylsilane (2344-80-1) → C11H14F2O2Si (1602574-20-8)

Guidance literature:

With potassium carbonate; sodium iodide; In N,N-dimethyl-formamide; at 65 ℃;

DOI:10.1016/j.bmcl.2014.03.096

Downstream raw materials:

1-{3,6-difluoro-2-[(3-methylbut-2-en-1-yl)oxy]phenyl}-3-N-Boc-methylaminoprop-2-yn-ol

hexacarbonyl[1-{3,6-difluoro-2-[(3-methylbut-2-en-1-yl)oxy]phenyl}-3-N-Boc-methylaminoprop-2-yn-ol]dicobalt

3,6-difluoro-2-[(3-methylbut-2-en-1-yl)oxy]benzaldehyde

C₁₁H₁₄F₂O₂Si

Refernces