Technology Process of 9-Benzyl-9-borabicyclo[3.3.1]nonane
There total 5 articles about 9-Benzyl-9-borabicyclo[3.3.1]nonane which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium peroxomonosulfate / methanol; water / 12 h / 0 - 20 °C / Inert atmosphere
2.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 - 0 °C / Inert atmosphere
2.2: 0 - 20 °C / Inert atmosphere
With
n-butyllithium; potassium peroxomonosulfate;
In
tetrahydrofuran; methanol; hexane; water;
DOI:10.1021/ol300672q
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 80 °C / Inert atmosphere
2.1: potassium peroxomonosulfate / methanol; water / 12 h / 0 - 20 °C / Inert atmosphere
3.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 - 0 °C / Inert atmosphere
3.2: 0 - 20 °C / Inert atmosphere
With
n-butyllithium; potassium peroxomonosulfate; potassium carbonate;
In
tetrahydrofuran; methanol; hexane; water; N,N-dimethyl-formamide;
DOI:10.1021/ol300672q
F,
Xi
