DIBROMOACETALDEHYDE DIETHYL ACETAL

Base Information

• Chemical Name: DIBROMOACETALDEHYDE DIETHYL ACETAL
• CAS No.: 761-17-1
• Molecular Formula: C6H12Br2O2
• Molecular Weight: 275.968
• Mol file: 761-17-1.mol

Synonyms:DIBROMOACETALDEHYDE DIETHYL ACETAL

Chemical Property of DIBROMOACETALDEHYDE DIETHYL ACETAL

Chemical Property:

• PSA: 18.46000
• LogP: 2.50140

Purity/Quality:

95+% ^*data from raw suppliers

DibromoacetaldehydeDiethylAcetal ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of DIBROMOACETALDEHYDE DIETHYL ACETAL

There total 9 articles about DIBROMOACETALDEHYDE DIETHYL ACETAL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

Bromoacetaldehyde diethyl acetal (2032-35-1) → 1,1-dibromo-2,2-diethoxy-ethane (761-17-1)

Guidance literature:

With bromine; In diethyl ether; at 20 ℃; for 20h; Inert atmosphere; Cooling with ice;

DOI:10.1002/anie.201811717

Reference yield:

bromine (7726-95-6) + 1,1,2-triethoxyethane (4819-77-6) → ethyl bromide (74-96-4) + ethanol (64-17-5) + 1,1-dibromo-2,2-diethoxy-ethane (761-17-1) + water (7732-18-5)

Guidance literature:

at 80 ℃;

Reference yield:

diethyl acetal (105-57-7,30846-29-8) → 1,1-dibromo-2,2-diethoxy-ethane (761-17-1)

Guidance literature:

With pyridine; at 10 - 15 ℃; Bromieren;

upstream raw materials:

diethyl acetal

diethyl ether

Bromoacetaldehyde diethyl acetal

paracetaldehyde

Downstream raw materials:

bromal

dibromoacetaldehyde

2,2-diethoxy-1,1,1-tribromo-ethane

ethyl dibromoacetate

Refernces