Technology Process of Silanamine, 1,1,1-trimethyl-
There total 9 articles about Silanamine, 1,1,1-trimethyl- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
(η5-C5Me5)Rh(2-pyridylphenyl)H; hydrogen;
In
tetrahydrofuran;
at 23 ℃;
for 120h;
under 3040.2 Torr;
Reagent/catalyst;
Catalytic behavior;
Inert atmosphere;
Schlenk technique;
DOI:10.1021/jacs.6b08009
- Guidance literature:
-
With
NaNH2;
In
tetrahydrofuran;
under N2, dropwise addn. of boron-compd. in THF to a -78°C cold soln. of NaNH2 in THF, warmed to room temp.; all volatiles pumped off, treated with petroleum ether;
- Guidance literature:
-
With
potassium amide;
In
ammonia;
byproducts: (C6H5)3CK;
DOI:10.1021/ja01156a116