3,4-Pyridinedicarboxylic acid, 5-methoxy-6-methyl-

Base Information

• Chemical Name: 3,4-Pyridinedicarboxylic acid, 5-methoxy-6-methyl-
• CAS No.: 7442-22-0
• Molecular Formula: C₉H₉NO₅
• Molecular Weight: 211.174
• Mol file: 7442-22-0.mol

Synonyms:3,4-Pyridinedicarboxylic acid, 5-methoxy-6-methyl-

Chemical Property of 3,4-Pyridinedicarboxylic acid, 5-methoxy-6-methyl-

Chemical Property:

• PSA: 96.72000
• LogP: 0.79500

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,4-Pyridinedicarboxylic acid, 5-methoxy-6-methyl-

There total 9 articles about 3,4-Pyridinedicarboxylic acid, 5-methoxy-6-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4,5-bis-hydroxymethyl-3-methoxy-2-methyl-pyridine (633-72-7) → 7-methoxy-6-methyl-1H-furo[3,4-c]pyridin-3-one (847020-95-5) + 5-methoxy-6-methyl-pyridine-3,4-dicarboxylic acid (7442-22-0)

Guidance literature:

With potassium hydroxide; potassium permanganate;

Reference yield:

7-methoxy-6-methyl-1H-furo[3,4-c]pyridin-3-one (847020-95-5) → 5-methoxy-6-methyl-pyridine-3,4-dicarboxylic acid (7442-22-0)

Guidance literature:

With barium dihydroxide; barium permanganate;

DOI:10.1021/ja01874a068

Reference yield:

5-hydroxy-6-methyl-3,4-pyridinedimethanol (65-23-6) → 5-methoxy-6-methyl-pyridine-3,4-dicarboxylic acid (7442-22-0)

Guidance literature:

Multi-step reaction with 2 steps

1: methanol; diethyl ether

2: aqueous Ba(MnO₄)2

With methanol; barium permanganate; diethyl ether;

DOI:10.1021/ja01874a067

upstream raw materials:

4-methoxy-3-methyl-isoquinoline

4,5-bis-hydroxymethyl-3-methoxy-2-methyl-pyridine

7-methoxy-6-methyl-1H-furo[3,4-c]pyridin-3-one

7-methoxy-6-methylfuro[3,4-c]pyridin-1(3H)-one