HOC₅H₃NCOOSn(C₆H₅CH₂)3

Base Information

• Chemical Name: HOC₅H₃NCOOSn(C₆H₅CH₂)3
• CAS No.: 1202633-59-7
• Molecular Formula: C₂₇H₂₅NO₃Sn
• Molecular Weight: 530.21
• Mol file: 1202633-59-7.mol

Synonyms:

Chemical Property of HOC₅H₃NCOOSn(C₆H₅CH₂)3

Chemical Property:

Purity/Quality:

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Technology Process of HOC₅H₃NCOOSn(C₆H₅CH₂)3

There total 1 articles about HOC₅H₃NCOOSn(C₆H₅CH₂)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

5-hydroxynicotinic acid (27828-71-3) + tribenzyltin(IV) chloride (3151-41-5) → HOC5H3NCOOSn(C6H5CH2)3 (1202633-59-7)

Guidance literature:

With sodium ethoxide; In methanol; 5-hydroxynicotinic acid and sodium ethoxide (1:1) added to soln. of CH3OH, stirred for 30 min, treated with 1 equiv. of Bn3SnCl, stirred for 12 h at 40°C; filtered, evapd.(vac.), recrystd.(ether), elem. anal.;

DOI:10.1016/j.jorganchem.2009.09.001

upstream raw materials:

5-hydroxynicotinic acid

tribenzyltin(IV) chloride

Refernces