D-glycero-D-manno-Heptonicacid, g-lactone

Base Information

• Chemical Name: D-glycero-D-manno-Heptonicacid, g-lactone
• CAS No.: 5329-44-2
• Molecular Formula: C7H12 O7
• Molecular Weight: 208.168
• Mol file: 5329-44-2.mol

Synonyms:NSC2554

Chemical Property of D-glycero-D-manno-Heptonicacid, g-lactone

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of D-glycero-D-manno-Heptonicacid, g-lactone

There total 2 articles about D-glycero-D-manno-Heptonicacid, g-lactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

D-Allose (2595-97-3) + sodium cyanide (143-33-9,25596-52-5) → D-glycero-D-altro-heptonic acid-4-lactone (89-67-8,3257-66-7,5329-44-2,10030-65-6,15397-07-6,15397-08-7,15397-09-8,22404-04-2,60046-25-5,92007-82-4) + D-glycero-D-allo-heptonic acid-4-lactone (89-67-8,3257-66-7,5329-44-2,10030-65-6,15397-07-6,15397-08-7,15397-09-8,22404-04-2,60046-25-5,92007-82-4)

Guidance literature:

With water; anschliessend Erhitzen der Reaktionsloesung unter vermindertem Druck;

DOI:10.1021/ja01628a075

Reference yield:

D-Allose (2595-97-3) + sodium cyanide (143-33-9,25596-52-5) → D-glycero-D-altro-heptonic acid-4-lactone (89-67-8,3257-66-7,5329-44-2,10030-65-6,15397-07-6,15397-08-7,15397-09-8,22404-04-2,60046-25-5,92007-82-4) + D-glycero-D-allo-heptonic acid-4-lactone (89-67-8,3257-66-7,5329-44-2,10030-65-6,15397-07-6,15397-08-7,15397-09-8,22404-04-2,60046-25-5,92007-82-4)

Guidance literature:

With water; anschliessend Erhitzen der Reaktionsloesung unter vermindertem Druck;

DOI:10.1021/ja01628a075

Reference yield:

D-glycero-D-manno-heptonic acid-4-lactone (5329-44-2) → volemitol (488-38-0)

Guidance literature:

Multi-step reaction with 2 steps

1: aqueous sulfuric acid; sodium-amalgam

2: Raney nickel; water / 100 °C / 154457 Torr / Hydrogenation

With sodium amalgam; sulfuric acid; water; nickel;

DOI:10.1021/ja01154a129

upstream raw materials:

D-Allose

sodium cyanide

Downstream raw materials:

(1R)-1-(1H-benzimidazol-2-yl)-D-altritol

D-Glycero-D-manno-heptonsaeure-phenylhydrazid

D-glycero-D-manno-heptose

D-glycero-D-manno-heptonic acid amide