Carbazol-4-one hydrochloride

Base Information

• Chemical Name: Carbazol-4-one hydrochloride
• CAS No.: 99614-70-7
• Molecular Formula: C₁₆H₂₀N₂O*ClH
• Molecular Weight: 292.809
• Mol file: 99614-70-7.mol

Synonyms:1,2,3,9-Tetrahydro-9-methyl-3-[(2-methylamino)methyl]-4H-carbazol-4-one;

Chemical Property of Carbazol-4-one hydrochloride

Chemical Property:

• Vapor Pressure: 6.1E-08mmHg at 25°C
• Boiling Point: 443.6 °C at 760 mmHg
• Flash Point: 222.1 °C
• PSA: 29.43000
• LogP: 0.73090

Purity/Quality:

99.9% ^*data from raw suppliers

3-[(DIMETHYLAMINO)METHYL]-1,2,3,9-TETRAHYDRO-9-METHYL-4H-CARBAZOL-4-ONE HYDROCHLORIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Carbazol-4-one hydrochloride

There total 1 articles about Carbazol-4-one hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 9-methyl-1,2,3,9-tetrahydro-4H-carbazol-4-one (27387-31-1,808754-65-6) + N,N-dimethylammonium chloride (506-59-2) → 3-[(dimethylamine)methyl]-1,2,3,9-tetrahydro-9-methyl-4H-carbazol-4-one hydrochloride (132659-89-3,99614-70-7) + 9-methyl-3-methylene-1,2,3,9-tetrahydro-4H-carbazol-4-one (99614-64-9)

Guidance literature:

With acetic acid; In water; toluene; at 100 - 105 ℃; for 3.5h; Product distribution / selectivity;

upstream raw materials:

formaldehyd

9-methyl-1,2,3,9-tetrahydro-4H-carbazol-4-one

N,N-dimethylammonium chloride

Refernces