Technology Process of <(5-Cyan-1-benzofuran-2-yl)methyl>triphenylphosphoniumchlorid
There total 5 articles about <(5-Cyan-1-benzofuran-2-yl)methyl>triphenylphosphoniumchlorid which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
xylene;
for 2h;
Heating;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 80 percent / N-methylpyrrolidine / 0.5 h / Heating
2: 95 percent / 1) NaHCO3, CaI2, NaBH4; 2) CaI2, NaBH4 / tetrahydrofuran / 1) 0 to 5 deg C, 1 h; 2) room temp., 2 h
3: 74 percent / pyridine, SOCl2 / diethyl ether / 4 h / Ambient temperature
4: 71 percent / xylene / 2 h / Heating
With
1-Methylpyrrolidine; pyridine; sodium tetrahydroborate; thionyl chloride; sodium hydrogencarbonate; calcium iodide;
In
tetrahydrofuran; diethyl ether; xylene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 95 percent / conc. H2SO4 / 15 h / Heating
2: 80 percent / N-methylpyrrolidine / 0.5 h / Heating
3: 95 percent / 1) NaHCO3, CaI2, NaBH4; 2) CaI2, NaBH4 / tetrahydrofuran / 1) 0 to 5 deg C, 1 h; 2) room temp., 2 h
4: 74 percent / pyridine, SOCl2 / diethyl ether / 4 h / Ambient temperature
5: 71 percent / xylene / 2 h / Heating
With
1-Methylpyrrolidine; pyridine; sodium tetrahydroborate; thionyl chloride; sulfuric acid; sodium hydrogencarbonate; calcium iodide;
In
tetrahydrofuran; diethyl ether; xylene;