Technology Process of C33H55(3)H3O2Si2
There total 8 articles about C33H55(3)H3O2Si2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dilithium tetrachlorocuprate;
In
tetrahydrofuran; diethyl ether;
at 20 ℃;
for 4h;
DOI:10.1002/jlcr.1840
- Guidance literature:
-
Multi-step reaction with 6 steps
1: dihydrogen peroxide; sodium hydroxide / water; toluene
2: carbon tetrabromide; triphenylphosphine / acetonitrile / 1 h / 20 °C / Cooling with ice
3: boron tribromide / dichloromethane; 1,2-dichloro-ethane / 1.5 h / Reflux
4: boron trifluoride diethyl etherate; magnesium sulfate / dichloromethane / 1 h / -40 °C / Inert atmosphere
5: 2,6-dimethylpyridine / dichloromethane / 20 °C
6: dilithium tetrachlorocuprate / tetrahydrofuran; diethyl ether / 4 h / 20 °C
With
2,6-dimethylpyridine; dilithium tetrachlorocuprate; carbon tetrabromide; boron trifluoride diethyl etherate; dihydrogen peroxide; boron tribromide; magnesium sulfate; triphenylphosphine; sodium hydroxide;
In
tetrahydrofuran; diethyl ether; dichloromethane; water; 1,2-dichloro-ethane; toluene; acetonitrile;
DOI:10.1002/jlcr.1840
- Guidance literature:
-
Multi-step reaction with 3 steps
1: boron trifluoride diethyl etherate; magnesium sulfate / dichloromethane / 1 h / -40 °C / Inert atmosphere
2: 2,6-dimethylpyridine / dichloromethane / 20 °C
3: dilithium tetrachlorocuprate / tetrahydrofuran; diethyl ether / 4 h / 20 °C
With
2,6-dimethylpyridine; dilithium tetrachlorocuprate; boron trifluoride diethyl etherate; magnesium sulfate;
In
tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1002/jlcr.1840
