(+/-)-α-truxillic acid monoamide

Base Information

• Chemical Name: (+/-)-α-truxillic acid monoamide
• CAS No.: 109212-92-2
• Molecular Formula: C₁₈H₁₇NO₃
• Molecular Weight: 295.338
• Mol file: 109212-92-2.mol

Synonyms:

Chemical Property of (+/-)-α-truxillic acid monoamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (+/-)-α-truxillic acid monoamide

There total 26 articles about (+/-)-α-truxillic acid monoamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-3-phenylacrylic acid (140-10-3) + cinnamamide (621-79-4,22031-64-7) → 1S,2S,3S,4S-truxillic acid monoamide (109212-92-2,109281-30-3)

Guidance literature:

for 720h; Irradiation;

DOI:10.1021/ja00185a036

Reference yield:

α-truxillic acid (4462-95-7) → truxillic acid monoamide (109212-92-2,109281-30-3) + 2,4-diphenyl-1,3-cyclobutanedicarboxamide (101792-96-5)

Guidance literature:

With 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide; In 1,4-dioxane; N,N-dimethyl-formamide; at 0 ℃; for 1h; Yield given;

DOI:10.1021/ja00185a036

Reference yield:

→ peritruxillic acid monoamide (109212-92-2,109281-30-3)

Guidance literature:

With ammonium hydroxide; at 110 ℃;

upstream raw materials:

2c,4t-diphenyl-cyclobutane-1r,3t-dicarboxylic acid diamide

α-truxillic acid

(+/-)-γ-truxillic acid monoamide

ε-truxillic acid diamide

Downstream raw materials:

(+/-)-γ-truxillic acid monoamide

ε-truxillic acid

ε-truxillic acid diamide

epitruxillic acid

Refernces