Technology Process of N,N'-[(phenylimino)di-4,1-phenylene]bis-(5-trifluoromethyl phthalimide)
There total 4 articles about N,N'-[(phenylimino)di-4,1-phenylene]bis-(5-trifluoromethyl phthalimide) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
5-trifluoromethylbenzofuran-1,3-dione; bis(4-aminophenyl)phenylamine;
In
tetrahydrofuran;
for 1h;
With
1,3-dimethyl-2-imidazolidinone;
for 4h;
Reflux;
DOI:10.1021/cm201665g
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / N,N-dimethyl acetamide / 0.5 h / 20 °C
1.2: 1 h / 100 °C
2.1: palladium on activated charcoal; hydrazine hydrate / ethanol / 12 h / Reflux
3.1: tetrahydrofuran / 1 h
3.2: 4 h / Reflux
With
palladium on activated charcoal; sodium hydride; hydrazine hydrate;
In
tetrahydrofuran; ethanol; N,N-dimethyl acetamide;
DOI:10.1021/cm201665g
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: acetyl chloride / 16 h / Reflux
2.1: tetrahydrofuran / 1 h
2.2: 4 h / Reflux
With
acetyl chloride;
In
tetrahydrofuran;
DOI:10.1021/cm201665g
