2,6-dichloro-4-methylphenyl methyl phosphorochloridothionate

Base Information

• Chemical Name: 2,6-dichloro-4-methylphenyl methyl phosphorochloridothionate
• CAS No.: 96790-20-4
• Molecular Formula: C₈H₈Cl₃O₂PS
• Molecular Weight: 305.549
• Mol file: 96790-20-4.mol

Synonyms:

Chemical Property of 2,6-dichloro-4-methylphenyl methyl phosphorochloridothionate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,6-dichloro-4-methylphenyl methyl phosphorochloridothionate

There total 2 articles about 2,6-dichloro-4-methylphenyl methyl phosphorochloridothionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

Mono-demethyl tolclofos-methyl → 2,6-dichloro-4-methylphenyl methyl phosphorochloridothionate (96790-20-4)

Guidance literature:

With phosphorus pentachloride; In dichloromethane; Ambient temperature;

Reference yield:

tolclofos-methyl (57018-04-9,78617-09-1) → 2,6-dichloro-4-methylphenyl methyl phosphorochloridothionate (96790-20-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 100 percent / potassium dimethyldithiocarbamate / ethanol / Ambient temperature

2: 33 percent / PCl₅ / CH₂Cl₂ / Ambient temperature

With phosphorus pentachloride; potassium dimethyldithiocarbamate; In ethanol; dichloromethane;

Reference yield:

D-2-phenylglycinol (56613-80-0) + 2,6-dichloro-4-methylphenyl methyl phosphorochloridothionate (96790-20-4) → (S)P(R)C-2-Methoxy-4-phenyl-1,3,2-oxazaphospholidine 2-sulfide + (R)P(R)C-2-Methoxy-4-phenyl-1,3,2-oxazaphospholidine 2-sulfide

Guidance literature:

In chloroform-d1; Rate constant; Ambient temperature;

upstream raw materials:

tolclofos-methyl

Refernces