C₁₇H₂₃N₅OSi

Base Information

• Chemical Name: C₁₇H₂₃N₅OSi
• CAS No.: 1315141-31-1
• Molecular Formula: C₁₇H₂₃N₅OSi
• Molecular Weight: 341.488
• Mol file: 1315141-31-1.mol

Synonyms:

Chemical Property of C₁₇H₂₃N₅OSi

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₇H₂₃N₅OSi

There total 3 articles about C₁₇H₂₃N₅OSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(2-methoxy-4-nitrophenyl)-4-methyl-1H-imidazole (958245-17-5) → C17H23N5OSi (1315141-31-1)

Guidance literature:

Multi-step reaction with 3 steps

1: 10% palladium on activated charcoal; hydrogen

2: sodium azide; sodium nitrite

3: copper(II) sulfate; sodium L-ascorbate / ethanol; water

With sodium azide; 10% palladium on activated charcoal; hydrogen; copper(II) sulfate; sodium L-ascorbate; sodium nitrite; In ethanol; water;

DOI:10.1016/j.bmcl.2011.04.089

Reference yield:

1-bromo-2-methoxy-4-nitrobenzene (77337-82-7) → C17H23N5OSi (1315141-31-1)

Guidance literature:

Multi-step reaction with 4 steps

1: potassium carbonate / N,N-dimethyl-formamide / Heating

2: 10% palladium on activated charcoal; hydrogen

3: sodium azide; sodium nitrite

4: copper(II) sulfate; sodium L-ascorbate / ethanol; water

With sodium azide; 10% palladium on activated charcoal; hydrogen; potassium carbonate; copper(II) sulfate; sodium L-ascorbate; sodium nitrite; In ethanol; water; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2011.04.089

Reference yield:

trimethyl(propargyl)silane (13361-64-3) + C11H11N5O (1315141-29-7) → C17H23N5OSi (1315141-31-1)

Guidance literature:

With copper(II) sulfate; sodium L-ascorbate; In ethanol; water;

DOI:10.1016/j.bmcl.2011.04.089

upstream raw materials:

1-(2-methoxy-4-nitrophenyl)-4-methyl-1H-imidazole

trimethyl(propargyl)silane

C₁₁H₁₁N₅O

1-bromo-2-methoxy-4-nitrobenzene

Refernces