C₁₆H₂₄O₄

Base Information

• Chemical Name: C₁₆H₂₄O₄
• CAS No.: 1310717-17-9
• Molecular Formula: C₁₆H₂₄O₄
• Molecular Weight: 280.364
• Mol file: 1310717-17-9.mol

Synonyms:

Chemical Property of C₁₆H₂₄O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₆H₂₄O₄

There total 1 articles about C₁₆H₂₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

4-bromobutyl benzyl ether (60789-54-0) + ethyl (R)-(+)-2,3-epoxypropanoate (4660-80-4,93264-11-0,111058-34-5,111058-33-4) → C16H24O4 (1310717-17-9)

Guidance literature:

4-bromobutyl benzyl ether; With magnesium; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

With copper(I) bromide dimethylsulfide complex; In tetrahydrofuran; at -78 ℃; Inert atmosphere;

ethyl (R)-(+)-2,3-epoxypropanoate; In tetrahydrofuran; regioselective reaction; Inert atmosphere;

DOI:10.1074/jbc.M110.211649

Reference yield:

C16H24O4 (1310717-17-9) → C37H44O10P2 (1310717-21-5)

Guidance literature:

Multi-step reaction with 2 steps

1.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / Inert atmosphere

2.1: 1H-tetrazole / dichloromethane / Inert atmosphere

2.2: Inert atmosphere

With 1H-tetrazole; palladium 10% on activated carbon; hydrogen; In dichloromethane; ethyl acetate;

DOI:10.1074/jbc.M110.211649

upstream raw materials:

4-bromobutyl benzyl ether

ethyl (R)-(+)-2,3-epoxypropanoate

Downstream raw materials:

C₃₇H₄₄O₁₀P₂

Refernces