Technology Process of 2,4,6-Triiodobenzene-1,3,5-tricarboxylic acid
There total 5 articles about 2,4,6-Triiodobenzene-1,3,5-tricarboxylic acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
1,3,5-triiodo-2,4-diacetoxymethyl-6-methyl-benzene;
With
sodium hydroxide; water;
at 90 ℃;
for 5h;
With
hydrogenchloride;
In
water;
pH=6 - 7;
With
potassium permanganate; magnesium sulfate;
In
water;
for 2h;
Product distribution / selectivity;
Heating / reflux;
- Guidance literature:
-
2,4,6-triiodomesitylene; acetic anhydride; acetic acid;
With
potassium permanganate; sulfuric acid;
at 40 - 50 ℃;
for 20 - 30h;
Acidic conditions;
With
sodium hydroxide;
In
water;
at 20 ℃;
Alkaline conditions;
With
sodium hydroxide; potassium permanganate; sulfuric acid; water;
more than 3 stages;
Product distribution / selectivity;
