1,10-bis-1,4,7,10-tetraoxadecane

Base Information

• Chemical Name: 1,10-bis-1,4,7,10-tetraoxadecane
• CAS No.: 130740-00-0
• Molecular Formula: C₂₄H₂₆O₈
• Molecular Weight: 442.466
• Mol file: 130740-00-0.mol

Synonyms:

Chemical Property of 1,10-bis-1,4,7,10-tetraoxadecane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,10-bis-1,4,7,10-tetraoxadecane

There total 2 articles about 1,10-bis-1,4,7,10-tetraoxadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

1,2-bis-(2-bromo-ethoxy)-ethane (31255-10-4) + p-Coumaric Acid (7400-08-0,50940-26-6) → 1,10-bis-1,4,7,10-tetraoxadecane (130740-00-0)

Guidance literature:

With sodium hydroxide; In ethanol; for 26h; Heating;

DOI:10.1246/bcsj.63.1623

Reference yield:

4-hydroxy-benzaldehyde (123-08-0,65581-83-1) → 1,10-bis-1,4,7,10-tetraoxadecane (130740-00-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 32.1 percent / piperidine / pyridine / 7 h / 100 °C

2: 23 percent / NaOH / aq. ethanol / 26 h / Heating

With piperidine; sodium hydroxide; In pyridine; ethanol;

DOI:10.1246/bcsj.63.1623

Reference yield:

1,10-bis-1,4,7,10-tetraoxadecane (130740-00-0) → 1,10-bisphenyl>-1,4,7,10-tetraoxadecane (201421-50-3)

Guidance literature:

With thionyl chloride; at 35 ℃; for 5h;

DOI:10.1246/bcsj.63.1623

upstream raw materials:

1,2-bis-(2-bromo-ethoxy)-ethane

p-Coumaric Acid

4-hydroxy-benzaldehyde

Downstream raw materials:

1,10-bisphenyl>-1,4,7,10-tetraoxadecane

Refernces