Technology Process of 2-(4-benzyloxy-3-methoxyphenyl)ethyl β-D-galactopyranoside
There total 6 articles about 2-(4-benzyloxy-3-methoxyphenyl)ethyl β-D-galactopyranoside which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium methylate;
In
methanol;
at 20 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: silver carbonate / diethyl ether; dichloromethane / 1 h / 20 °C / Inert atmosphere; Molecular sieve
1.2: 14 h / 20 °C / Inert atmosphere; Darkness
2.1: sodium methylate / methanol / 2 h / 20 °C
With
sodium methylate; silver carbonate;
In
methanol; diethyl ether; dichloromethane;
1.1: |Koenigs-Knorr Glycosidation / 1.2: |Koenigs-Knorr Glycosidation;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium carbonate / acetone / 1 h / Inert atmosphere; Reflux
2.1: copper(I) bromide / methanol; N,N-dimethyl-formamide
2.2: 2.5 h / 110 °C
3.1: silver carbonate / diethyl ether; dichloromethane / 1 h / 20 °C / Inert atmosphere; Molecular sieve
3.2: 14 h / 20 °C / Inert atmosphere; Darkness
4.1: sodium methylate / methanol / 2 h / 20 °C
With
sodium methylate; potassium carbonate; silver carbonate; copper(I) bromide;
In
methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetone;
3.1: |Koenigs-Knorr Glycosidation / 3.2: |Koenigs-Knorr Glycosidation;