N-benzenesulphonyl-N,2,3-trimethyl-6-quinoxalinamine

Base Information

• Chemical Name: N-benzenesulphonyl-N,2,3-trimethyl-6-quinoxalinamine
• CAS No.: 109671-50-3
• Molecular Formula: C₁₇H₁₇N₃O₂S
• Molecular Weight: 327.407
• Mol file: 109671-50-3.mol

Synonyms:

Chemical Property of N-benzenesulphonyl-N,2,3-trimethyl-6-quinoxalinamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-benzenesulphonyl-N,2,3-trimethyl-6-quinoxalinamine

There total 2 articles about N-benzenesulphonyl-N,2,3-trimethyl-6-quinoxalinamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3-dimethyl-6-quinoxalinamine (7576-88-7) → N-benzenesulphonyl-N,2,3-trimethyl-6-quinoxalinamine (109671-50-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 86 percent / pyridine / 0.67 h / Heating

2: 84 percent / Bu₄N⁺OH^-, NaOH / CH₂Cl₂ / 0.83 h / Heating

With pyridine; sodium hydroxide; tetra(n-butyl)ammonium hydroxide; In dichloromethane;

Reference yield:

benzenesulfonyl chloride (98-09-9) → N-benzenesulphonyl-N,2,3-trimethyl-6-quinoxalinamine (109671-50-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 86 percent / pyridine / 0.67 h / Heating

2: 84 percent / Bu₄N⁺OH^-, NaOH / CH₂Cl₂ / 0.83 h / Heating

With pyridine; sodium hydroxide; tetra(n-butyl)ammonium hydroxide; In dichloromethane;

Reference yield: 69.0%

N-benzenesulphonyl-N,2,3-trimethyl-6-quinoxalinamine (109671-50-3) → N,2,3-trimethyl-6-quinoxalinamine (60639-47-6)

Guidance literature:

With sulfuric acid; for 0.416667h; Heating;

upstream raw materials:

2,3-dimethyl-6-quinoxalinamine

benzenesulfonyl chloride

Downstream raw materials:

N,2,3-trimethyl-5-nitro-6-quinoxalinamine

N,2,3-trimethyl-6-quinoxalinamine

2-amino-3,7,8-trimethylimidazo[4,5-f]quinoxaline

Refernces