Technology Process of C21H37BO8Si3
There total 3 articles about C21H37BO8Si3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex;
In
5,5-dimethyl-1,3-cyclohexadiene; toluene;
at 20 ℃;
for 1h;
Overall yield = 59 %; Overall yield = 106 mg;
DOI:10.1039/c2cc37438b
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dichloromethane / 3 h / 20 °C / Molecular sieve; Inert atmosphere
2: platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex / toluene; 5,5-dimethyl-1,3-cyclohexadiene / 1 h / 20 °C
With
platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex;
In
5,5-dimethyl-1,3-cyclohexadiene; dichloromethane; toluene;
DOI:10.1039/c2cc37438b
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dichloromethane / 3 h / 20 °C / Molecular sieve; Inert atmosphere
2: platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex / toluene; 5,5-dimethyl-1,3-cyclohexadiene / 1 h / 20 °C
With
platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex;
In
5,5-dimethyl-1,3-cyclohexadiene; dichloromethane; toluene;
DOI:10.1039/c2cc37438b