C₅₈H₇₀N₈O₄

Base Information

• Chemical Name: C₅₈H₇₀N₈O₄
• CAS No.: 102393-34-0
• Molecular Formula: C₅₈H₇₀N₈O₄
• Molecular Weight: 943.245
• Mol file: 102393-34-0.mol

Synonyms:

Chemical Property of C₅₈H₇₀N₈O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₈H₇₀N₈O₄

There total 21 articles about C₅₈H₇₀N₈O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,5-dimethyl-2-ethoxycarbonyl-1H-pyrrole (2199-44-2) → C58H70N8O4 (102393-34-0)

Guidance literature:

Multi-step reaction with 10 steps

1: SnCl₂ / CH₂Cl₂; nitromethane / Ambient temperature

2: B₂H₆ / tetrahydrofuran

3: PhCH₂ONa / Heating

4: H₂, triethylamine / 10 percent Pd/C / tetrahydrofuran / Ambient temperature

5: dimethylformamide / Heating

6: POCl₃ / CH₂Cl₂

7: NaHCO₃ / H₂O / Heating

8: cyclohexylamine / toluene / Heating

9: SO₂Cl₂ / CH₂Cl₂ / Ambient temperature

10: glacial acetic acid / 80 °C

With sulfuryl dichloride; hydrogen; sodium hydrogencarbonate; cyclohexylamine; acetic acid; triethylamine; sodium phenyl-methanolate; tin(ll) chloride; diborane; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; nitromethane; dichloromethane; water; N,N-dimethyl-formamide; toluene;

Reference yield:

1-methylbuta-1,3-diene (2004-70-8,17410-45-6,25212-15-1,64940-84-7) → C58H70N8O4 (102393-34-0)

Guidance literature:

Multi-step reaction with 11 steps

1: Zn, acetic acid

2: SnCl₂ / CH₂Cl₂; nitromethane / Ambient temperature

3: B₂H₆ / tetrahydrofuran

4: PhCH₂ONa / Heating

5: H₂, triethylamine / 10 percent Pd/C / tetrahydrofuran / Ambient temperature

6: dimethylformamide / Heating

7: POCl₃ / CH₂Cl₂

8: NaHCO₃ / H₂O / Heating

9: cyclohexylamine / toluene / Heating

10: SO₂Cl₂ / CH₂Cl₂ / Ambient temperature

11: glacial acetic acid / 80 °C

With sulfuryl dichloride; hydrogen; sodium hydrogencarbonate; cyclohexylamine; acetic acid; triethylamine; sodium phenyl-methanolate; tin(ll) chloride; diborane; zinc; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; nitromethane; dichloromethane; water; N,N-dimethyl-formamide; toluene;

Reference yield:

1,4-bis(chloromethyl)-2,3,5,6-tetramethylbenzene (3022-16-0) → C58H70N8O4 (102393-34-0)

Guidance literature:

Multi-step reaction with 19 steps

1: 1.) Na / 1.) ethanol; 2.) ethanol, reflux, 0.5 h

2: H₂O, KOH / Heating

3: 94.7 percent / quinoline / 0.33 h / Heating

4: 89.4 percent / cc. H₂SO₄ / toluene

5: 89.6 percent / B₂H₆ / tetrahydrofuran

6: 91.2 percent / 48 percent HBr / H₂O / 0.5 h / Heating

7: 97 percent / ethanol / 4 h / Heating

8: 98 percent / H₂O, KOH / ethanol / Heating

9: SOCl₂ / Heating

10: SnCl₂ / CH₂Cl₂; nitromethane / Ambient temperature

11: B₂H₆ / tetrahydrofuran

12: PhCH₂ONa / Heating

13: H₂, triethylamine / 10 percent Pd/C / tetrahydrofuran / Ambient temperature

14: dimethylformamide / Heating

15: POCl₃ / CH₂Cl₂

16: NaHCO₃ / H₂O / Heating

17: cyclohexylamine / toluene / Heating

18: SO₂Cl₂ / CH₂Cl₂ / Ambient temperature

19: glacial acetic acid / 80 °C

With quinoline; potassium hydroxide; thionyl chloride; sulfuryl dichloride; sulfuric acid; water; hydrogen bromide; hydrogen; sodium; sodium hydrogencarbonate; cyclohexylamine; acetic acid; triethylamine; sodium phenyl-methanolate; tin(ll) chloride; diborane; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; nitromethane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;

upstream raw materials:

ethyl 4-ethyl-3-methylpyrrole-2-carboxylate

3-{5-Chloromethyl-4-[4-(4-{4-[2-chloromethyl-5-(2,2-dicyano-vinyl)-4-methyl-1H-pyrrol-3-yl]-butyl}-2,3,5,6-tetramethyl-phenyl)-butyl]-3-methyl-1H-pyrrol-2-yl}-2-cyano-acrylonitrile

3,5-dimethyl-2-ethoxycarbonyl-1H-pyrrole

1-methylbuta-1,3-diene

Downstream raw materials:

C₄₆H₆₂N₄O₂

C₄₈H₆₂N₄O₆

Refernces