Si(NHNHC₆H₅)4(SnCl₄)

Base Information

• Chemical Name: Si(NHNHC₆H₅)4(SnCl₄)
• CAS No.: 122953-85-9
• Molecular Formula: C₂₄H₂₈Cl₄N₈SiSn
• Molecular Weight: 717.147
• Mol file: 122953-85-9.mol

Synonyms:

Chemical Property of Si(NHNHC₆H₅)4(SnCl₄)

Chemical Property:

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Technology Process of Si(NHNHC₆H₅)4(SnCl₄)

There total 1 articles about Si(NHNHC₆H₅)4(SnCl₄) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

(CF3CH2O)3Si(NHNHC6H5) + tin(IV) chloride (7646-78-8) → Si(NHNHC6H5)4(SnCl4) (122953-85-9) + tetrakis(2,2,2-trifluoroethoxy)silane (338-39-6)

Guidance literature:

In Petroleum ether; dropwise addn. of soln. of SnCl4 in petroleum ether (40-60°C) to soln. of 1-trialkoxysilyl 2-phenylhydrazine (equimolar amts., 0 to -10°C, under dry nitrogen), ppt. filtered in a cold atm. of dry N2; washed, dried under reduced pressure; elem. anal.;

DOI:10.1016/S0020-1693(00)80899-3

upstream raw materials:

tin(IV) chloride