1,4-Dioxa-7,11-dithiacyclotridecane

Base Information

• Chemical Name: 1,4-Dioxa-7,11-dithiacyclotridecane
• CAS No.: 115663-30-4
• Molecular Formula: C9H18O2S2
• Molecular Weight: 222.373
• Mol file: 115663-30-4.mol

Synonyms:

Chemical Property of 1,4-Dioxa-7,11-dithiacyclotridecane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,4-Dioxa-7,11-dithiacyclotridecane

There total 1 articles about 1,4-Dioxa-7,11-dithiacyclotridecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

propane‐1,3‐diyl dicarbamimidothioate dihydrobromide (5442-32-0,64039-23-2) + triethylene glycol di-(p-toluenesulfonate) (19249-03-7) → 8,11-dioxa-1,5-dithiacyclotridecane (115663-30-4)

Guidance literature:

With potassium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In benzene; for 7h; Ambient temperature;

upstream raw materials:

propane‐1,3‐diyl dicarbamimidothioate dihydrobromide

triethylene glycol di-(p-toluenesulfonate)

Refernces

• 1、 Singh, Paramjit,Kumar, Manoj,Singh, Harjit. "Synthesis of Oxygen and Sulphur Containing Crown Compounds under Solid-Liquid Phase Transfer Catalysis". . p. 861 - 862. Retrieved 2007/10/02.