Technology Process of C44H46O2
There total 9 articles about C44H46O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
2,4,6-trimethylphenyl bromide;
With
n-butyllithium;
In
tetrahydrofuran; hexane;
at -78 ℃;
for 0.666667h;
C35H34O2;
In
tetrahydrofuran; hexane;
at -78 ℃;
for 0.333333h;
DOI:10.1002/anie.201208058
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: silver nitrate; N-Bromosuccinimide / acetone / 3 h / 20 °C
2.1: copper(l) chloride; hydroxylamine hydrochloride; propylamine / ethanol / 12 h / 20 °C
3.1: pyridinium chlorochromate / dichloromethane / 4 h / 20 °C / Molecular sieve
4.1: n-butyllithium / hexane; tetrahydrofuran / 0.67 h / -78 °C
4.2: 0.33 h / -78 °C
With
propylamine; N-Bromosuccinimide; n-butyllithium; hydroxylamine hydrochloride; silver nitrate; pyridinium chlorochromate; copper(l) chloride;
In
tetrahydrofuran; ethanol; hexane; dichloromethane; acetone;
2.1: |Cadiot-Chodkiewicz Coupling;
DOI:10.1002/anie.201208058
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: copper(l) chloride; hydroxylamine hydrochloride; propylamine / ethanol / 12 h / 20 °C
2.1: pyridinium chlorochromate / dichloromethane / 4 h / 20 °C / Molecular sieve
3.1: n-butyllithium / hexane; tetrahydrofuran / 0.67 h / -78 °C
3.2: 0.33 h / -78 °C
With
propylamine; n-butyllithium; hydroxylamine hydrochloride; pyridinium chlorochromate; copper(l) chloride;
In
tetrahydrofuran; ethanol; hexane; dichloromethane;
1.1: |Cadiot-Chodkiewicz Coupling;
DOI:10.1002/anie.201208058
