o-Methylsulfon-phenylaethylenglykol

Base Information

• Chemical Name: o-Methylsulfon-phenylaethylenglykol
• CAS No.: 92474-86-7
• Molecular Formula: C₉H₁₂O₄S
• Molecular Weight: 216.258
• Mol file: 92474-86-7.mol

Synonyms:

Chemical Property of o-Methylsulfon-phenylaethylenglykol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of o-Methylsulfon-phenylaethylenglykol

There total 6 articles about o-Methylsulfon-phenylaethylenglykol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ω-Acetoxy-o-methylsulfon-acetophenon (111211-66-6) → o-Methylsulfon-phenylaethylenglykol (92474-86-7)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether;

Reference yield:

1,2-Diacetoxy-1-(o-methylsulfon-phenyl)-aethan (106478-01-7) → o-Methylsulfon-phenylaethylenglykol (92474-86-7)

Guidance literature:

With sodium methylate; In methanol;

Reference yield:

2-(methylsulfonyl)benzoic acid (33963-55-2) → o-Methylsulfon-phenylaethylenglykol (92474-86-7)

Guidance literature:

Multi-step reaction with 4 steps

1: SOCl₂

2: diethyl ether

3: KOAc

4: LiAlH₄ / diethyl ether

With lithium aluminium tetrahydride; thionyl chloride; potassium acetate; In diethyl ether;

upstream raw materials:

ω-Acetoxy-o-methylsulfon-acetophenon

1,2-Diacetoxy-1-(o-methylsulfon-phenyl)-aethan

2-(methylsulfonyl)benzoic acid

o-Methylsulfon-ω-diazo-acetophenon

Downstream raw materials:

2-methylsulphonylbenzaldehyde

o-Methylsulfon-propiophenon