1-benzyl 3-ethyl 2,2-dimethylmalonate

Base Information

• Chemical Name: 1-benzyl 3-ethyl 2,2-dimethylmalonate
• CAS No.: 1347024-62-7
• Molecular Formula: C₁₄H₁₈O₄
• Molecular Weight: 250.295
• Mol file: 1347024-62-7.mol

Synonyms:

Chemical Property of 1-benzyl 3-ethyl 2,2-dimethylmalonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-benzyl 3-ethyl 2,2-dimethylmalonate

There total 1 articles about 1-benzyl 3-ethyl 2,2-dimethylmalonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

benzyl bromide (100-39-0) + cesium formate (3495-36-1) + methyl methacrylate (97-63-2,9003-42-3) → 1-benzyl 3-ethyl 2,2-dimethylmalonate (1347024-62-7)

Guidance literature:

cesium formate; methyl methacrylate; With C₂₂H₃₁F₃GeO₃P₂PdS; In N,N-dimethyl-formamide; at 80 ℃; for 6h; Inert atmosphere; Green chemistry;

benzyl bromide; With potassium carbonate; sodium iodide; In N,N-dimethyl-formamide; at 20 ℃; for 12h; regioselective reaction; Inert atmosphere; Green chemistry;

DOI:10.1039/c7cc01377a

upstream raw materials:

benzyl bromide

cesium formate

methyl methacrylate

Refernces