t-butyl phenyl phosphinic trifluoroacetate

Base Information

• Chemical Name: t-butyl phenyl phosphinic trifluoroacetate
• CAS No.: 169783-28-2
• Molecular Formula: C₁₂H₁₄F₃O₃P
• Molecular Weight: 294.21
• Mol file: 169783-28-2.mol

Synonyms:

Chemical Property of t-butyl phenyl phosphinic trifluoroacetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of t-butyl phenyl phosphinic trifluoroacetate

There total 2 articles about t-butyl phenyl phosphinic trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

P-(1,1-dimethylethyl)-P-phenylphosphinoselenoic acid Se-methyl ester (113502-18-4) + mercury(II) trifluoroacetate (13257-51-7) → t-butyl phenyl phosphinic trifluoroacetate (169783-28-2)

Guidance literature:

In acetonitrile;

Reference yield:

t-butyl phenyl selenophosphinic acid (51584-27-1,51584-28-2) → t-butyl phenyl phosphinic trifluoroacetate (169783-28-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 98 percent / Et₃N / CH₂Cl₂

2: 92 percent / acetonitrile

With triethylamine; In dichloromethane; acetonitrile;

Reference yield: 82.0%

t-butyl phenyl phosphinic trifluoroacetate (169783-28-2) → t-butyl(phenyl)phosphinic acid (4923-86-8)

Guidance literature:

With methanol; for 0.25h;

upstream raw materials:

P-(1,1-dimethylethyl)-P-phenylphosphinoselenoic acid Se-methyl ester

mercury(II) trifluoroacetate

t-butyl phenyl selenophosphinic acid

Downstream raw materials:

t-butyl(phenyl)phosphinic acid

Refernces