Technology Process of Platinum, tris(triphenylphosphine)-
There total 64 articles about Platinum, tris(triphenylphosphine)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Me2(CH2=CH)SiOSiMe2(CH=CH2); triphenylphosphine;
In
water;
byproducts: C2H4, C4H6, HCl; H2PtCl6*xH2O was heated with excess (Me2ViSi)2O at 50°C for 4 h, cooled, neutralized with NaHCO3, filtered, PPh3 added;
- Guidance literature:
-
With
potassium hydroxide;
In
ethanol; water;
at 65 ℃;
for 0.5h;
Inert atmosphere;
DOI:10.1002/chem.201601292
- Guidance literature:
-
With
triphenylphosphine;
In
tetrahydrofuran;
byproducts: ZnCl2; N2-atmosphere; refluxing 3 equiv. of PPh3 with PdCl2 (1 h), addn. of Zn-dust, refluxing for 3 h; filtration, evapn. (vac.), washing (EtOH); elem. anal.;
DOI:10.1016/S0020-1693(00)95469-0