Benzeneacetaldehyde, 3-chloro-a-(3-chlorophenyl)-

Base Information

• Chemical Name: Benzeneacetaldehyde, 3-chloro-a-(3-chlorophenyl)-
• CAS No.: 135807-10-2
• Molecular Formula: C14H10Cl2O
• Molecular Weight: 265.139
• Mol file: 135807-10-2.mol

Synonyms:

Chemical Property of Benzeneacetaldehyde, 3-chloro-a-(3-chlorophenyl)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzeneacetaldehyde, 3-chloro-a-(3-chlorophenyl)-

There total 7 articles about Benzeneacetaldehyde, 3-chloro-a-(3-chlorophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C15H12Cl2O → bis-(3-chlorophenyl)acetaldehyde (135807-10-2)

Guidance literature:

With perchloric acid; In 1,4-dioxane; water; at 90 ℃; for 0.5h;

Reference yield:

1,1-bis-(3-chlorophenyl)-2-methoxyethanol + (3-chlorophenyl)magnesium bromide (36229-42-2) → bis-(3-chlorophenyl)acetaldehyde (135807-10-2)

Guidance literature:

With sodium carbonate; In tetrahydrofuran; formic acid; ethyl acetate;

Reference yield:

1,1-bis-(3-chlorophenyl)-2-methoxyethanol + methyl methoxyacetate (6290-49-9) + (3-chlorophenyl)magnesium bromide (36229-42-2) → bis-(3-chlorophenyl)acetaldehyde (135807-10-2)

Guidance literature:

With sodium carbonate; In tetrahydrofuran; formic acid; ethyl acetate;

upstream raw materials:

3,3-bis-(3-chloro-phenyl)-oxirane-2-carboxylic acid

bis(3-chlorophenyl)methanone

methyl methoxyacetate

(3-chlorophenyl)magnesium bromide

Refernces

• 1、 Knutsen, Lars J. S.,Andersen, Knud Erik,Lau, Jesper,Lundt, Behrend F.,Henry, Rodger F.,Morton, Howard E.,N?rum, Lars,Petersen, Hans,Stephensen, Henrik,Suzdak, Peter D.,Swedberg, Michael D. B.,Thomsen, Christian,S?rensen, Per O.. "Synthesis of novel GABA uptake inhibitors. 3. Diaryloxime and diarylvinyl ether derivatives of nipecotic acid and guvacine as anticonvulsant agents". . p. 3447 - 3462. Retrieved 2007/10/03.
• 2、 -. "Isoindolone derivatives, their preparation and the pharmaceutical compositions containing them". . . Retrieved 2008/06/13.