acetoxy-pyruvaldehyde bis-(2,4-dinitro-phenylhydrazone)

Base Information

• Chemical Name: acetoxy-pyruvaldehyde bis-(2,4-dinitro-phenylhydrazone)
• CAS No.: 101451-22-3
• Molecular Formula: C₁₇H₁₄N₈O₁₀
• Molecular Weight: 490.346
• Mol file: 101451-22-3.mol

Synonyms:

Chemical Property of acetoxy-pyruvaldehyde bis-(2,4-dinitro-phenylhydrazone)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of acetoxy-pyruvaldehyde bis-(2,4-dinitro-phenylhydrazone)

There total 4 articles about acetoxy-pyruvaldehyde bis-(2,4-dinitro-phenylhydrazone) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3-diacetoxyacetone (6946-10-7) + (2,4-dinitro-phenyl)-hydrazine (119-26-6) → acetoxy-pyruvaldehyde bis-(2,4-dinitro-phenylhydrazone) (101451-22-3)

Guidance literature:

With acetic acid;

DOI:10.1021/ja01315a029

Reference yield:

(2,4-dinitro-phenyl)-hydrazine (119-26-6) → acetoxy-pyruvaldehyde bis-(2,4-dinitro-phenylhydrazone) (101451-22-3)

Guidance literature:

Multi-step reaction with 2 steps

1: aqueous HCl

2: pyridine; acetic acid

With pyridine; hydrogenchloride; acetic acid;

DOI:10.1021/jo01107a012

Reference yield:

acetic anhydride (108-24-7) + hydroxy-pyruvaldehyde bis-(2,4-dinitro-phenylhydrazone) (1060-83-9) → acetoxy-pyruvaldehyde bis-(2,4-dinitro-phenylhydrazone) (101451-22-3)

Guidance literature:

With pyridine; acetic acid;

DOI:10.1021/jo01107a012

upstream raw materials:

acetic anhydride

hydroxy-pyruvaldehyde bis-(2,4-dinitro-phenylhydrazone)

1,3-diacetoxyacetone

(2,4-dinitro-phenyl)-hydrazine