o-acetylaminobenzyl benzoate

Base Information

• Chemical Name: o-acetylaminobenzyl benzoate
• CAS No.: 129384-16-3
• Molecular Formula: C₁₆H₁₅NO₃
• Molecular Weight: 269.3
• Mol file: 129384-16-3.mol

Synonyms:

Chemical Property of o-acetylaminobenzyl benzoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of o-acetylaminobenzyl benzoate

There total 5 articles about o-acetylaminobenzyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

2-nitrobenzyl benzoate (110786-18-0) + acetic anhydride (108-24-7) → o-acetylaminobenzyl benzoate (129384-16-3)

Guidance literature:

With 10% Pd/C; hydrogen; In toluene; for 3h;

DOI:10.1016/j.bmc.2008.03.056

Reference yield:

N-acetyl-O-acetyl-2-aminobenzyl alcohol (83326-80-1) → o-acetylaminobenzyl benzoate (129384-16-3)

Guidance literature:

Multi-step reaction with 2 steps

1: NaOH-solution

2: NaOH-solution

With sodium hydroxide;

Reference yield:

2-(hydroxymethyl)benzenaminium hydrochloride → o-acetylaminobenzyl benzoate (129384-16-3)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium acetate

2: NaOH-solution

3: NaOH-solution

With sodium hydroxide; sodium acetate;

upstream raw materials:

2-acetamidobenzyl alcohol

benzoyl chloride

benzoic acid methyl ester

2-Aminobenzyl alcohol

Refernces

• 1、 Arai, Kenji,Tamura, Shohei,Masumizu, Tatsuya,Kawai, Ken-Ichi,Nakajima, Shoichi,Ueda, Akira. "A novel electrochemical method for benzoylation of aminoalcohols with methyl benzoates at room temperature". . p. 903 - 907. Retrieved 2007/10/02.