1-(4,5-dichloro-2-nitro-anilino)-1-deoxy-D-arabitol

Base Information

• Chemical Name: 1-(4,5-dichloro-2-nitro-anilino)-1-deoxy-D-arabitol
• CAS No.: 117776-56-4
• Molecular Formula: C₁₁H₁₄Cl₂N₂O₆
• Molecular Weight: 341.148
• Mol file: 117776-56-4.mol

Synonyms:

Chemical Property of 1-(4,5-dichloro-2-nitro-anilino)-1-deoxy-D-arabitol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(4,5-dichloro-2-nitro-anilino)-1-deoxy-D-arabitol

There total 6 articles about 1-(4,5-dichloro-2-nitro-anilino)-1-deoxy-D-arabitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

L-arabinose (5328-37-0) → 1-(4,5-dichloro-2-nitro-anilino)-1-deoxy-L-arabitol (117776-56-4)

Guidance literature:

Multi-step reaction with 2 steps

1: Raney nickel; ammonia / 85 °C / 102971 Torr / Hydrogenation

With ammonia; nickel;

DOI:10.1021/ja01168a014

Reference yield:

D-Arabinose (10323-20-3) → 1-(4,5-dichloro-2-nitro-anilino)-1-deoxy-D-arabitol (117776-56-4)

Guidance literature:

Multi-step reaction with 2 steps

1: Raney nickel; ammonia / 85 °C / 102971 Torr / Hydrogenation

With ammonia; nickel;

DOI:10.1021/ja01145a109

Reference yield:

L-1-amino-1-deoxyarabitinol (42015-12-3) + 1,2-dichloro-4,5-dinitrobenzene (6306-39-4) → 1-(4,5-dichloro-2-nitro-anilino)-1-deoxy-L-arabitol (117776-56-4)

Guidance literature:

DOI:10.1021/ja01168a014

upstream raw materials:

D-Ribamin

1,2-dichloro-4,5-dinitrobenzene

1,2-dichloro-benzene

L-1-amino-1-deoxyarabitinol

Downstream raw materials:

1-(2-amino-4,5-dichloro-anilino)-1-deoxy-D-ribitol