6-chloro-9-(2-chloro-6-fluorobenzyl) purine

Base Information Edit

Chemical Name:6-chloro-9-(2-chloro-6-fluorobenzyl) purine
CAS No.:72564-76-2
Molecular Formula:C₁₂H₇Cl₂FN₄
Molecular Weight:297.119
Hs Code.:
Mol file:72564-76-2.mol

Synonyms:

Suppliers and Price of 6-chloro-9-(2-chloro-6-fluorobenzyl) purine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-chloro-9-(2-chloro-6-fluorobenzyl) purine Edit

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of 6-chloro-9-(2-chloro-6-fluorobenzyl) purine

There total 3 articles about 6-chloro-9-(2-chloro-6-fluorobenzyl) purine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 72564-77-3
9-(2-chloro-6-fluorobenzyl)purin-6(1H)-one

: 72564-76-2
6-chloro-9-(2-chloro-6-fluorobenzyl) purine

Guidance literature:: With tri-n-propylamine; trichlorophosphate; for 0.666667h; Heating;

Reference yield:

: 68220-26-8
2-(bromomethyl)-1-chloro-3-fluorobenzene

: 87-42-3,111055-92-6
6-chloro-7H-purine

: 72564-76-2
6-chloro-9-(2-chloro-6-fluorobenzyl) purine

Guidance literature:: With potassium carbonate; In dimethyl sulfoxide; for 39h; Ambient temperature;
DOI:10.1021/jm00400a019

Reference yield:

: 55779-18-5
9-(2-chloro-6-fluorobenzyl)adenine

: 72564-76-2
6-chloro-9-(2-chloro-6-fluorobenzyl) purine

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / sodium nitrite / acetic acid; H₂O / 2 h / 60 - 70 °C

2: 67 percent / phosphoryl chloride, tripropyl amine / 0.67 h / Heating

With tri-n-propylamine; sodium nitrite; trichlorophosphate; In water; acetic acid;