Technology Process of C7(2)H14O2
There total 5 articles about C7(2)H14O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 86.5 percent / LiAlD4 / diethyl ether / 8 h / Heating
2: 83.7 percent / red phosphorous, Br2 / 85 - 90 °C
3: 1.) EtONa / 1.) EtOH, 50 deg C, 1 h, 2.) EtOH, 30 deg C, 6 h
4: 1.) D2O, NaOD, 2.) D2SO4 / 1.) reflux, 6 h, 2.) reflux, 4.5 h
With
phosphorus; lithium aluminium deuteride; deuteriated sodium hydroxide; bromine; water-d2; sodium ethanolate; sulfuric acid-d2;
In
diethyl ether;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) D2O, NaOD, 2.) D2SO4 / 1.) reflux, 6 h, 2.) reflux, 4.5 h
2: 86.5 percent / LiAlD4 / diethyl ether / 8 h / Heating
3: 83.7 percent / red phosphorous, Br2 / 85 - 90 °C
4: 1.) EtONa / 1.) EtOH, 50 deg C, 1 h, 2.) EtOH, 30 deg C, 6 h
5: 1.) D2O, NaOD, 2.) D2SO4 / 1.) reflux, 6 h, 2.) reflux, 4.5 h
With
phosphorus; lithium aluminium deuteride; deuteriated sodium hydroxide; bromine; water-d2; sodium ethanolate; sulfuric acid-d2;
In
diethyl ether;
- Guidance literature:
-
With
deuteriated sodium hydroxide; water-d2; sulfuric acid-d2;
Yield given. Multistep reaction;
1.) reflux, 6 h, 2.) reflux, 4.5 h;