Pd(CH₃)PN₃(CH₂)6C₆H₃(CH(CH₃)2)2NCHC₆H₂OCl₂

Base Information

• Chemical Name: Pd(CH₃)PN₃(CH₂)6C₆H₃(CH(CH₃)2)2NCHC₆H₂OCl₂
• CAS No.: 630416-13-6
• Molecular Formula: C₂₆H₃₅Cl₂N₄OPPd
• Molecular Weight: 627.89
• Mol file: 630416-13-6.mol

Synonyms:

Chemical Property of Pd(CH₃)PN₃(CH₂)6C₆H₃(CH(CH₃)2)2NCHC₆H₂OCl₂

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of Pd(CH₃)PN₃(CH₂)6C₆H₃(CH(CH₃)2)2NCHC₆H₂OCl₂

There total 1 articles about Pd(CH₃)PN₃(CH₂)6C₆H₃(CH(CH₃)2)2NCHC₆H₂OCl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.8%

(N,N,N',N'-tetramethylethylenediamine)dimethylpalladium(II) + 4,6-dichloro-2-[[(2,6-diisopropylphenyl)imino]methyl]phenol (210882-40-9) + (1,3,5-triaza-7-phosphaadamantane) (53597-69-6) → Pd(CH3)PN3(CH2)6C6H3(CH(CH3)2)2NCHC6H2OCl2 (630416-13-6)

Guidance literature:

In methanol; toluene; ligand in MeOH was introduced into Schlenk flask with Pd-complex in toluene at -30°C, second ligand in toluene was slowly added, stirred for 30 min under Ar, warmed to room temp., stirred overnight; solvent was removed in vacuo, cooled to -78°C, pentane was added,filtered, washed with pentane at -78°C; elem. anal.;

DOI:10.1021/ic0341284

upstream raw materials:

4,6-dichloro-2-[[(2,6-diisopropylphenyl)imino]methyl]phenol

(1,3,5-triaza-7-phosphaadamantane)

Refernces