Technology Process of 1ζ-acetoxy-6-methoxy-2-(p-methoxyphenyl)-2-methyl-1,2,3,4-tetrahydronaphthalene
There total 9 articles about 1ζ-acetoxy-6-methoxy-2-(p-methoxyphenyl)-2-methyl-1,2,3,4-tetrahydronaphthalene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine;
for 12h;
Ambient temperature;
DOI:10.1071/CH9842279
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 99 percent / H2, TEA / PtO / propan-2-ol / 760 Torr / Ambient temperature
2: 99 percent / sulfuryl chloride / CCl4 / 12 h / Ambient temperature
3: 25 percent / tetrahydrofuran; benzene / 3 h / Heating
4: 99 percent / LiAlH4 / diethyl ether / 15 h / Heating
5: 81 percent / pyridine / 12 h / Ambient temperature
With
pyridine; lithium aluminium tetrahydride; sulfuryl dichloride; TEA; hydrogen;
platinum(II) oxide;
In
tetrahydrofuran; tetrachloromethane; diethyl ether; isopropyl alcohol; benzene;
DOI:10.1071/CH9842279
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 99 percent / sulfuryl chloride / CCl4 / 12 h / Ambient temperature
2: 25 percent / tetrahydrofuran; benzene / 3 h / Heating
3: 99 percent / LiAlH4 / diethyl ether / 15 h / Heating
4: 81 percent / pyridine / 12 h / Ambient temperature
With
pyridine; lithium aluminium tetrahydride; sulfuryl dichloride;
In
tetrahydrofuran; tetrachloromethane; diethyl ether; benzene;
DOI:10.1071/CH9842279
