Technology Process of N,N'-1,2-acenaphthylenediylidene bis(2,6-dimethyl aniline) palladium(II)(methyl)(κ2-CH(OAc)Et) tetra(3,5-trifluoromethyl ph
There total 1 articles about N,N'-1,2-acenaphthylenediylidene bis(2,6-dimethyl aniline) palladium(II)(methyl)(κ2-CH(OAc)Et) tetra(3,5-trifluoromethyl ph which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
dichloromethane;
(Ar), Pd complex in dry box cooled to 0°C, slowly treated with dry CH2Cl2 and vinyl acetate , stirred for 2 h, warmed to 20°C; chromy.(SiO2 - Et2O), crystd.(CH2Cl2-pentane) at -30°C, elem. anal., NMR;
Kinetics;
DOI:10.1021/ja045969s